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Search for "structural characterization" in Full Text gives 77 result(s) in Beilstein Journal of Nanotechnology.

Nanomedicines against Chagas disease: a critical review

  • Maria Jose Morilla,
  • Kajal Ghosal and
  • Eder Lilia Romero

Beilstein J. Nanotechnol. 2024, 15, 333–349, doi:10.3762/bjnano.15.30

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  • the reasons can be summarized as follows: Difficult scale-up, structural characterization, and conservation: The structure of nanomedicines is much more complex than that of drugs with low molecular weight. Because of that, nanomedicines are considered as non-biological complex drugs (NBCDs). NBCDs
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Published 27 Mar 2024

Upscaling the urea method synthesis of CoAl layered double hydroxides

  • Camilo Jaramillo-Hernández,
  • Víctor Oestreicher,
  • Martín Mizrahi and
  • Gonzalo Abellán

Beilstein J. Nanotechnol. 2023, 14, 927–938, doi:10.3762/bjnano.14.76

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  • The α-Co layered hydroxide synthesis was carried out at room temperature by using the epoxide route for a period of 48 h under constant stirring with solutions of [CoCl2] = 10 mM and [NaCl] = 100 mM, in the presence of glycidol, [Gly] = 500 mM. Chemical and structural characterization Powder X-ray
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Published 11 Sep 2023

Silver-based SERS substrates fabricated using a 3D printed microfluidic device

  • Phommachith Sonexai,
  • Minh Van Nguyen,
  • Bui The Huy and
  • Yong-Ill Lee

Beilstein J. Nanotechnol. 2023, 14, 793–803, doi:10.3762/bjnano.14.65

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  • with an increase in the concentration of reactants. Structural characterization of the SERS substrate In Supporting Information File 1, Figure S10a shows the SEM image of the SAM of Ag NPs on the surface of methanol, while Figure S10b displays the image of the PS substrate after covering with the Ag
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Published 21 Jul 2023

In situ magnesiothermic reduction synthesis of a Ge@C composite for high-performance lithium-ion batterie anodes

  • Ha Tran Huu,
  • Ngoc Phi Nguyen,
  • Vuong Hoang Ngo,
  • Huy Hoang Luc,
  • Minh Kha Le,
  • Minh Thu Nguyen,
  • My Loan Phung Le,
  • Hye Rim Kim,
  • In Young Kim,
  • Sung Jin Kim,
  • Van Man Tran and
  • Vien Vo

Beilstein J. Nanotechnol. 2023, 14, 751–761, doi:10.3762/bjnano.14.62

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  • composites using magnesiothermic reduction was reported. Structural characterization indicates a good binding between Ge and carbon matrix after the in situ synthesis, which alleviates the structural stress induced by volume change and increases the conduction of electrons and ions in the composite
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Published 26 Jun 2023

On the use of Raman spectroscopy to characterize mass-produced graphene nanoplatelets

  • Keith R. Paton,
  • Konstantinos Despotelis,
  • Naresh Kumar,
  • Piers Turner and
  • Andrew J. Pollard

Beilstein J. Nanotechnol. 2023, 14, 509–521, doi:10.3762/bjnano.14.42

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  • produced and purchased. The publication of international standards is a key step in this process, such as recent publications on nomenclature [6] and structural characterization [7]. The measurement methods described in these standards, however, can be time-consuming and expensive. As the range of
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Published 24 Apr 2023

A novel approach to pulsed laser deposition of platinum catalyst on carbon particles for use in polymer electrolyte membrane fuel cells

  • Bogusław Budner,
  • Wojciech Tokarz,
  • Sławomir Dyjak,
  • Andrzej Czerwiński,
  • Bartosz Bartosewicz and
  • Bartłomiej Jankiewicz

Beilstein J. Nanotechnol. 2023, 14, 190–204, doi:10.3762/bjnano.14.19

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  • graphitized carbon material is a higher barrier to be overcome for the gases and the water generated in reactions occurring in the cell. Conclusion The fabrication of an efficient catalyst based on carbon particles with low Pt loading was successfully achieved by using the PLD method. The structural
  • characterization of fabricated catalysts by HAADF, EDX, and TEM showed a greater uniformity and a higher dispersion of the PtNPs on the carbon supports compared to the reference catalysts. However, only in the case of catalysts based on the commercial carbon support Vulcan XC-72R maximum cell power densities
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Published 02 Feb 2023

Upper critical magnetic field in NbRe and NbReN micrometric strips

  • Zahra Makhdoumi Kakhaki,
  • Antonio Leo,
  • Federico Chianese,
  • Loredana Parlato,
  • Giovanni Piero Pepe,
  • Angela Nigro,
  • Carla Cirillo and
  • Carmine Attanasio

Beilstein J. Nanotechnol. 2023, 14, 45–51, doi:10.3762/bjnano.14.5

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  • ]. NbReN films also present a polycrystalline nature with a moderate texture. In this case, it was possible to interpret the results of the structural characterization only by assuming for NbReN the same unit cell as that of NbRe [4]. However, detailed knowledge of its structural and microscopic properties
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Published 05 Jan 2023

In search of cytotoxic selectivity on cancer cells with biogenically synthesized Ag/AgCl nanoparticles

  • Mitzi J. Ramírez-Hernández,
  • Mario Valera-Zaragoza,
  • Omar Viñas-Bravo,
  • Ariana A. Huerta-Heredia,
  • Miguel A. Peña-Rico,
  • Erick A. Juarez-Arellano,
  • David Paniagua-Vega,
  • Eduardo Ramírez-Vargas and
  • Saúl Sánchez-Valdes

Beilstein J. Nanotechnol. 2022, 13, 1505–1519, doi:10.3762/bjnano.13.124

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  • comparison to monocytes. Keywords: cancer cells; cytotoxic behavior; green synthesis; pineapple extract; silver chloride nanoparticles; silver nanoparticles; structural characterization; Introduction The study of metallic nanoparticle synthesis by green methods is gaining importance, especially in cases
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Published 13 Dec 2022

Recent advances in green carbon dots (2015–2022): synthesis, metal ion sensing, and biological applications

  • Aisha Kanwal,
  • Naheed Bibi,
  • Sajjad Hyder,
  • Arif Muhammad,
  • Hao Ren,
  • Jiangtao Liu and
  • Zhongli Lei

Beilstein J. Nanotechnol. 2022, 13, 1068–1107, doi:10.3762/bjnano.13.93

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Published 05 Oct 2022

Self-assembly of C60 on a ZnTPP/Fe(001)–p(1 × 1)O substrate: observation of a quasi-freestanding C60 monolayer

  • Guglielmo Albani,
  • Michele Capra,
  • Alessandro Lodesani,
  • Alberto Calloni,
  • Gianlorenzo Bussetti,
  • Marco Finazzi,
  • Franco Ciccacci,
  • Alberto Brambilla,
  • Lamberto Duò and
  • Andrea Picone

Beilstein J. Nanotechnol. 2022, 13, 857–864, doi:10.3762/bjnano.13.76

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  • sample. The full width at half maximum (FWHM) energy resolution of the UPS experiment is 0.05 eV. Results and Discussion Figure 1a and Figure 1b report the structural characterization of the ZnTPP/Fe(001)–p(1 × 1)O sample in the reciprocal and in direct space, respectively. The low-energy electron
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Published 30 Aug 2022

Hierarchical Bi2WO6/TiO2-nanotube composites derived from natural cellulose for visible-light photocatalytic treatment of pollutants

  • Zehao Lin,
  • Zhan Yang and
  • Jianguo Huang

Beilstein J. Nanotechnol. 2022, 13, 745–762, doi:10.3762/bjnano.13.66

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  • ), EDTA-2Na (0.1 M), and p-BQ (5.0 mM) were also put into the initial RhB pollutant solution to capture •OH, h+, and •O2− species, respectively, generated during the photocatalytic degradation of RhB. Results and Discussion Structural characterization As shown in Figure 1, the Bi2WO6/TiO2-NT
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Published 04 Aug 2022

Surfactant-free syntheses and pair distribution function analysis of osmium nanoparticles

  • Mikkel Juelsholt,
  • Jonathan Quinson,
  • Emil T. S. Kjær,
  • Baiyu Wang,
  • Rebecca Pittkowski,
  • Susan R. Cooper,
  • Tiffany L. Kinnibrugh,
  • Søren B. Simonsen,
  • Luise Theil Kuhn,
  • María Escudero-Escribano and
  • Kirsten M. Ø. Jensen

Beilstein J. Nanotechnol. 2022, 13, 230–235, doi:10.3762/bjnano.13.17

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  • conditions to obtain Os NPs for further studies. Transmission electron microscopy images from samples synthesized with these parameter sets are shown in Figure 1. The small size of the nanoparticles challenges conventional structural characterization methods such as X-ray diffraction analysis (XRD). Here, we
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Published 16 Feb 2022

Electrical, electrochemical and structural studies of a chlorine-derived ionic liquid-based polymer gel electrolyte

  • Ashish Gupta,
  • Amrita Jain,
  • Manju Kumari and
  • Santosh K. Tripathi

Beilstein J. Nanotechnol. 2021, 12, 1252–1261, doi:10.3762/bjnano.12.92

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  • ionic liquid [BDiMIM][Cl], the host polymer PVdF-HFP, and the salt magnesium perchlorate (Mg(ClO4)2) were used to prepare polymer electrolyte films. The synthesized films were characterized by different microscopic and electrochemical techniques. Results and Discussion Structural characterization The
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Published 18 Nov 2021

A Au/CuNiCoS4/p-Si photodiode: electrical and morphological characterization

  • Adem Koçyiğit,
  • Adem Sarılmaz,
  • Teoman Öztürk,
  • Faruk Ozel and
  • Murat Yıldırım

Beilstein J. Nanotechnol. 2021, 12, 984–994, doi:10.3762/bjnano.12.74

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  • at a wavelength of 400–1100 nm. C–V measurements were carried out on a Keithley 4200 SCS. Results and Discussion Structural characterization Crystal structure, phase, and purity of the produced nanocrystals were investigated by XRD analysis. The XRD pattern of the nanocrystals is shown in Figure 2a
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Published 02 Sep 2021

Highly sensitive detection of estradiol by a SERS sensor based on TiO2 covered with gold nanoparticles

  • Andrea Brognara,
  • Ili F. Mohamad Ali Nasri,
  • Beatrice R. Bricchi,
  • Andrea Li Bassi,
  • Caroline Gauchotte-Lindsay,
  • Matteo Ghidelli and
  • Nathalie Lidgi-Guigui

Beilstein J. Nanotechnol. 2020, 11, 1026–1035, doi:10.3762/bjnano.11.87

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  • of all the spectra. The spectra presented here are the average of four spectra taken at different locations of each sample. Results and Discussion Sample growth and structural characterization Morphology Nanostructured TiO2 films with hierarchical micrometer/nanometer-scale morphology and tuned
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Published 14 Jul 2020

Simulations of the 2D self-assembly of tripod-shaped building blocks

  • Łukasz Baran,
  • Wojciech Rżysko and
  • Edyta Słyk

Beilstein J. Nanotechnol. 2020, 11, 884–890, doi:10.3762/bjnano.11.73

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  • diffraction pattern and average association number. Keywords: 2D materials; coarse-grained model; molecular simulations; self-assembly; structural characterization; tripod building blocks; Introduction On-surface synthesis is a newly developing field in chemistry that aims at making use of solid surfaces as
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Published 08 Jun 2020

Correction: An advanced structural characterization of templated meso-macroporous carbon monoliths by small- and wide-angle scattering techniques

  • Felix M. Badaczewski,
  • Marc O. Loeh,
  • Torben Pfaff,
  • Dirk Wallacher,
  • Daniel Clemens and
  • Bernd M. Smarsly

Beilstein J. Nanotechnol. 2020, 11, 678–679, doi:10.3762/bjnano.11.54

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Published 22 Apr 2020

An advanced structural characterization of templated meso-macroporous carbon monoliths by small- and wide-angle scattering techniques

  • Felix M. Badaczewski,
  • Marc O. Loeh,
  • Torben Pfaff,
  • Dirk Wallacher,
  • Daniel Clemens and
  • Bernd M. Smarsly

Beilstein J. Nanotechnol. 2020, 11, 310–322, doi:10.3762/bjnano.11.23

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  • , in this study advanced structural characterization methods are used to quantify the microstructure and pore structure of carbon monoliths based on different kinds of carbon precursors, namely a graphitizable pitch and a non-graphitizable resin. This coherent analysis helps to understand the impact of
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Published 10 Feb 2020

Nanosecond resistive switching in Ag/AgI/PtIr nanojunctions

  • Botond Sánta,
  • Dániel Molnár,
  • Patrick Haiber,
  • Agnes Gubicza,
  • Edit Szilágyi,
  • Zsolt Zolnai,
  • András Halbritter and
  • Miklós Csontos

Beilstein J. Nanotechnol. 2020, 11, 92–100, doi:10.3762/bjnano.11.9

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  • following the method of Kumar and co-workers [36]. The Ag films were evaporated on standard Si/SiO2 wafers using a 12 nm thick Ti sticking layer. The structural characterization of the thin film samples was carried out by Rutherford backscattering spectrometry (RBS) using an ion beam of 3500 keV 4He
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Published 08 Jan 2020

Recent progress in perovskite solar cells: the perovskite layer

  • Xianfeng Dai,
  • Ke Xu and
  • Fanan Wei

Beilstein J. Nanotechnol. 2020, 11, 51–60, doi:10.3762/bjnano.11.5

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  • ][41][42][43][44][45][46][47][48][49][50][51]. Structural characterization and morphology. (a) Schematic illustration of the structure of the 2D/3D PSCs. (b) XRD patterns as a function of the 2D perovskite doping concentration and (c) UV–vis absorption spectra of the (EDBEPbI4)x(MAPbI3)1−x films. (d–g
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Published 06 Jan 2020

Optimization and performance of nitrogen-doped carbon dots as a color conversion layer for white-LED applications

  • Tugrul Guner,
  • Hurriyet Yuce,
  • Didem Tascioglu,
  • Eren Simsek,
  • Umut Savaci,
  • Aziz Genc,
  • Servet Turan and
  • Mustafa M. Demir

Beilstein J. Nanotechnol. 2019, 10, 2004–2013, doi:10.3762/bjnano.10.197

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  • per hour as the operating conditions of the electrospinning process. Owing to the potential difference between the syringe tip and the collector aluminum foil, the N-CDots were confined into sub-micrometer fibers by electrospinning. Results and Discussion Structural characterization of the N-CDots
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Published 15 Oct 2019

Novel hollow titanium dioxide nanospheres with antimicrobial activity against resistant bacteria

  • Carol López de Dicastillo,
  • Cristian Patiño,
  • María José Galotto,
  • Yesseny Vásquez-Martínez,
  • Claudia Torrent,
  • Daniela Alburquenque,
  • Alejandro Pereira and
  • Juan Escrig

Beilstein J. Nanotechnol. 2019, 10, 1716–1725, doi:10.3762/bjnano.10.167

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  • and titanium dioxide, and after a calcination process, hollow nanospheres were obtained with a radius of approximately 345 nm and shell thickness of 17 nm. The structural characterization was performed using electron microscopy, and X-ray diffraction and small-angle X-ray diffraction evidenced an
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Published 19 Aug 2019

Hierarchically structured 3D carbon nanotube electrodes for electrocatalytic applications

  • Pei Wang,
  • Katarzyna Kulp and
  • Michael Bron

Beilstein J. Nanotechnol. 2019, 10, 1475–1487, doi:10.3762/bjnano.10.146

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  • . Structural characterization The nanostructured electrodes were examined via SEM employing an ESEM XI 30 FEG (Philips, Germany) instrument to characterize the morphology and structural properties. The average particle size and size distribution of Fe nanoparticles were determined by examining the size of 200
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Published 24 Jul 2019

Alloyed Pt3M (M = Co, Ni) nanoparticles supported on S- and N-doped carbon nanotubes for the oxygen reduction reaction

  • Stéphane Louisia,
  • Yohann R. J. Thomas,
  • Pierre Lecante,
  • Marie Heitzmann,
  • M. Rosa Axet,
  • Pierre-André Jacques and
  • Philippe Serp

Beilstein J. Nanotechnol. 2019, 10, 1251–1269, doi:10.3762/bjnano.10.125

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  • produced by the reference Pt3Co/CB is higher than for all the Pt3Co samples and most of the Pt3Ni catalysts prepared in this study. Thus, the H2O2 production is not an obstacle for using these catalysts for PEMFC applications. Structural characterization of the best catalysts For a better understanding of
  • there is a better interaction between the Ni and the N-CNTHT than the Co and the N-CNT. The catalysts were then filtered, washed with deionized water and dried for 24 hours at 80 °C. The same structural characterization was performed on the washed Pt3Co/N-CNT catalyst. The results of the XPS analysis
  • micrographs of the carbon supports are given in Supporting Information File 1, Figure S1. The CNTs, N-CNTs and S-CNTs have mean external diameters of 15 ± 5, 18 ± 8, and 15 ± 7 nm, respectively. The specific surface area (SSA) of these materials ranged between 150 m2/g (CNTs) and 190 m2/g (S-CNTs). Structural
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Published 21 Jun 2019

Green fabrication of lanthanide-doped hydroxide-based phosphors: Y(OH)3:Eu3+ nanoparticles for white light generation

  • Tugrul Guner,
  • Anilcan Kus,
  • Mehmet Ozcan,
  • Aziz Genc,
  • Hasan Sahin and
  • Mustafa M. Demir

Beilstein J. Nanotechnol. 2019, 10, 1200–1210, doi:10.3762/bjnano.10.119

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  • (OH)3. Results and Discussion Structural characterization of Y(OH)3:Eu3+ particles Figure 1a presents the X-ray diffraction pattern of representative Y(OH)3:Eu3+ particles having 7.5% dopant ratio (Y(OH)3:7.5% Eu3+) prepared at various reaction times. The pattern of the starting material (i.e
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Published 07 Jun 2019
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